5-Amino-1MQ

Certificate of Analysis & Complete Test Results

✓ Verified & Certified
Test Date
Jan 30, 2026
Batch Number
110069
Purity Level
99.54%

Certificate of Analysis

High-Performance Liquid Chromatography

Client: Peptides Canada
Sample Name: DSIP (Delta Sleep-Inducing Peptide)
Batch #: 110069
Report Date: 06/22/2025
Test: Purity
Receipt Date: 06/20/2025
Analysis Date: 06/22/2025
Matrix: Powder
Number of samples: 1
Purity: 99.54%

Research-grade specification: ≥95.0% — this batch exceeds specification.

Date File 110069_MS2_posneg_ DSIP _Lot110069_purity.d Sample Name DSIP _Lot110069_purity
Sample Type Sample Position P4-65
Instrument Name LCMS-7800 Series Username -
Acq Method DSIP _purity_5mg.m Acquired 06/22/2025 02:40:00 PM
IRM Calibration Status Calibrated Time (UTC-07:00)
Comment Sample test for purity of DSIP batch 110069 DA Method SignalToNoiseCheckout.m
Sample Group Test Batch 6 Info. -
Stream Name LC1 Acquisition 06/22/2025 02:40:00 PM
Acquisition SW Version 6400 Series Triple Quadrupole B.09.00 (89037.0) Time (Local) (UTC-07:00)

Peak List

Time Area % Area
3.12 min 5476.2 99.54 %
5.27 min 25.1 0.46 %

* determined as DSIP based on retention time

Note: Percent area between two compounds is not quantitative due to variable extinction coefficients.

Test Screen

UV Chromatogram:

Identity: DSIP

(Other names: Delta Sleep-Inducing Peptide, δ-Sleep-Inducing Peptide, Nonapeptide DSIP)

CAS: 62568-57-4

Data

Mass Spectrum

MSMS ID — head to tail database matching

Mass Spectrum Peptide Envelope encompasses the 1-3 positive change states conferring Peptide Mass

DSIP

Expected Mass: 850.9

Observed Mass: 850.9

Reviewed and approved by:

Herman Lelie

Pepslab.ca LLC. All test results are the responsibility of the client. This report relates only to the samples tested. The analyses were performed except as indicated. Samples are within quality control criteria and area specifications unless noted.